      Table 1.  Crystal data and structure refinement for AMB3. 
  
  
      Identification code               amb3 
  
      Empirical formula                 C33 H40 N O5 P 
  
      Formula weight                    561.63 
  
      Temperature                       293(2) K 
  
      Wavelength                        0.71073 A 
  
      Crystal system, space group       Triclinic,  P-1 
  
      Unit cell dimensions              a = 10.084(4) A   alpha = 94.75(2) deg. 
                                        b = 10.784(4) A    beta = 102.88(5) deg. 
                                        c = 13.878(6) A   gamma = 94.62(3) deg. 
  
      Volume                            1458.5(10) A^3 
  
      Z, Calculated density             2,  1.279 Mg/m^3 
  
      Absorption coefficient            0.137 mm^-1 
  
      F(000)                            600 
  
      Crystal size                      0.16 x 0.12 x 0.10 mm 
  
      Theta range for data collection   1.51 to 19.98 deg. 
  
      Limiting indices                  0<=h<=9, -10<=k<=10, -13<=l<=13 
  
      Reflections collected / unique    2930 / 2722 [R(int) = 0.0146] 
  
      Completeness to theta = 0.50      0.0 % 
  
      Absorption correction             Empirical via \y scans 
  
      Max. and min. transmission        0.9865 and 0.9785 
  
      Refinement method                 Full-matrix least-squares on F^2 
  
      Data / restraints / parameters    2722 / 0 / 406 
  
      Goodness-of-fit on F^2            1.034 
  
      Final R indices [I>2sigma(I)]     R1 = 0.0465, wR2 = 0.1334 
  
      R indices (all data)              R1 = 0.0556, wR2 = 0.1432 
  
      Largest diff. peak and hole       0.212 and -0.203 e.A^-3 
  
         Table 2.  Atomic coordinates ( x 10^4) and equivalent isotropic 
         displacement parameters (A^2 x 10^3) for AMB3. 
         U(eq) is defined as one third of the trace of the orthogonalized 
         Uij tensor. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          P             793(1)       6055(1)       7589(1)       55(1) 
          N           -2540(3)       5160(3)       9002(2)       63(1) 
          C           -1595(4)       5276(3)       8542(3)       58(1) 
          C(1)        -2544(4)       6110(3)       9766(2)       58(1) 
          C(2)        -3785(4)       6514(3)       9835(2)       63(1) 
          C(3)        -3854(4)       7468(3)      10533(3)       64(1) 
          C(4)        -2664(4)       7967(3)      11219(3)       64(1) 
          C(5)        -1452(4)       7537(4)      11165(3)       72(1) 
          C(6)        -1378(4)       6614(4)      10442(3)       68(1) 
          C(7)        -6153(5)       7765(5)       9850(4)       97(2) 
          C(8)        -7166(8)       8740(11)      9927(7)       80(2) 
          C(8A)       -6890(40)      8420(30)     10090(30)     300(40) 
          C(9)        -8186(7)       9851(9)      10972(6)      102(3) 
          C(9A)       -7750(110)    10190(90)     11030(70)    1100(200) 
          C(10)       -7498(9)      10895(7)      11612(7)      159(3) 
          C(11)       -5765(8)      11486(5)      13065(6)      140(2) 
          C(12)       -4935(8)      10925(6)      13908(5)      150(2) 
          C(13)       -4247(17)      9092(14)     13129(19)     190(13) 
          C(13A)      -3832(18)      9935(18)     12891(11)     117(5) 
          C(14)       -3295(7)       8657(6)      12672(4)      129(2) 
          O(1)        -4998(3)       7983(3)      10616(2)       97(1) 
          O(2)        -7521(5)       8778(6)      10802(4)       91(1) 
          O(2A)       -6901(12)      9594(12)     10635(10)      99(3) 
          O(3)        -6779(4)      10561(3)      12530(3)      121(1) 
          O(4)        -3666(14)     10213(10)     13531(11)     126(3) 
          O(4A)       -4612(10)      9828(9)      13661(6)       95(2) 
          O(5)        -2681(3)       8948(2)      11909(2)       81(1) 
          C(111)       -389(3)       4595(3)       7247(2)       51(1) 
          C(112)      -1428(3)       4361(3)       7756(2)       52(1) 
          C(113)      -2286(3)       3233(3)       7517(3)       64(1) 
          C(114)      -2139(4)       2366(3)       6785(3)       71(1) 
          C(115)      -1142(4)       2597(3)       6271(3)       66(1) 
          C(116)       -267(3)       3695(3)       6508(2)       60(1) 
          C(121)       2192(3)       5696(3)       7031(2)       54(1) 
          C(122)       3224(4)       5109(3)       7594(3)       71(1) 
          C(123)       4350(4)       4841(4)       7247(4)       89(1) 
          C(124)       4479(4)       5157(4)       6337(4)       94(1) 
          C(125)       3482(5)       5736(4)       5765(3)       85(1) 
          C(126)       2355(4)       6015(3)       6110(3)       68(1) 
          C(131)        -76(3)       7123(3)       6758(2)       54(1) 
          C(132)        363(4)       8386(3)       6958(3)       76(1) 
          C(133)       -242(5)       9248(4)       6372(4)       93(1) 
          C(134)      -1315(5)       8870(4)       5591(3)       84(1) 
          C(135)      -1772(4)       7621(4)       5388(3)       83(1) 
          C(136)      -1166(4)       6752(3)       5972(3)       69(1) 
         ________________________________________________________________ 
  
           Table 3.  Bond lengths [A] and angles [deg] for AMB3. 
           _____________________________________________________________ 
  
            P-C(121)                      1.807(4) 
            P-C(131)                      1.832(3) 
            P-C(111)                      1.857(3) 
            N-C                           1.264(4) 
            N-C(1)                        1.413(4) 
            C-C(112)                      1.456(5) 
            C(1)-C(6)                     1.371(5) 
            C(1)-C(2)                     1.378(5) 
            C(2)-C(3)                     1.371(5) 
            C(3)-O(1)                     1.343(4) 
            C(3)-C(4)                     1.391(5) 
            C(4)-C(5)                     1.357(5) 
            C(4)-O(5)                     1.370(4) 
            C(5)-C(6)                     1.372(5) 
            C(7)-C(8A)                    1.15(4) 
            C(7)-O(1)                     1.380(5) 
            C(7)-C(8)                     1.537(12) 
            C(8)-C(8A)                    0.50(3) 
            C(8)-O(2A)                    1.257(16) 
            C(8)-O(2)                     1.340(10) 
            C(8A)-O(2)                    1.33(5) 
            C(8A)-O(2A)                   1.42(4) 
            C(9)-C(9A)                    0.53(13) 
            C(9)-C(10)                    1.404(9) 
            C(9)-O(2)                     1.412(9) 
            C(9)-O(2A)                    1.510(14) 
            C(9A)-C(10)                   1.04(11) 
            C(9A)-O(2A)                   1.30(5) 
            C(9A)-O(2)                    1.57(7) 
            C(10)-O(3)                    1.409(8) 
            C(11)-O(3)                    1.402(6) 
            C(11)-C(12)                   1.482(8) 
            C(12)-O(4A)                   1.291(10) 
            C(12)-O(4)                    1.699(16) 
            C(13)-C(13A)                  1.078(17) 
            C(13)-O(4A)                   1.18(2) 
            C(13)-O(4)                    1.321(19) 
            C(13)-C(14)                   1.36(2) 
            C(13A)-O(4)                   0.887(11) 
            C(13A)-O(4A)                  1.467(17) 
            C(13A)-C(14)                  1.552(18) 
            C(14)-O(5)                    1.386(6) 
            O(2)-O(2A)                    1.108(11) 
            O(4)-O(4A)                    1.067(11) 
            C(111)-C(116)                 1.386(4) 
            C(111)-C(112)                 1.406(4) 
            C(112)-C(113)                 1.405(5) 
            C(113)-C(114)                 1.364(5) 
            C(114)-C(115)                 1.375(5) 
            C(115)-C(116)                 1.388(5) 
            C(121)-C(122)                 1.386(5) 
            C(121)-C(126)                 1.392(5) 
            C(122)-C(123)                 1.371(5) 
            C(123)-C(124)                 1.366(6) 
            C(124)-C(125)                 1.363(6) 
            C(125)-C(126)                 1.373(5) 
            C(131)-C(136)                 1.371(5) 
            C(131)-C(132)                 1.383(5) 
            C(132)-C(133)                 1.375(5) 
            C(133)-C(134)                 1.359(6) 
            C(134)-C(135)                 1.373(5) 
            C(135)-C(136)                 1.381(5) 
  
            C(121)-P-C(131)             102.16(15) 
            C(121)-P-C(111)             102.66(15) 
            C(131)-P-C(111)             102.31(14) 
            C-N-C(1)                    117.1(3) 
            N-C-C(112)                  123.7(3) 
            C(6)-C(1)-C(2)              119.6(3) 
            C(6)-C(1)-N                 122.7(3) 
            C(2)-C(1)-N                 117.7(3) 
            C(3)-C(2)-C(1)              120.7(3) 
            O(1)-C(3)-C(2)              125.1(3) 
            O(1)-C(3)-C(4)              115.9(3) 
            C(2)-C(3)-C(4)              119.1(3) 
            C(5)-C(4)-O(5)              119.1(3) 
            C(5)-C(4)-C(3)              119.8(3) 
            O(5)-C(4)-C(3)              120.9(3) 
            C(4)-C(5)-C(6)              121.0(3) 
            C(1)-C(6)-C(5)              119.8(3) 
            C(8A)-C(7)-O(1)             103.5(15) 
            C(8A)-C(7)-C(8)              14(2) 
            O(1)-C(7)-C(8)              111.8(5) 
            C(8A)-C(8)-O(2A)             98(5) 
            C(8A)-C(8)-O(2)              78(6) 
            O(2A)-C(8)-O(2)              50.4(6) 
            C(8A)-C(8)-C(7)              33(6) 
            O(2A)-C(8)-C(7)             120.4(8) 
            O(2)-C(8)-C(7)              111.4(7) 
            C(8)-C(8A)-C(7)             133(8) 
            C(8)-C(8A)-O(2)              80(6) 
            C(7)-C(8A)-O(2)             146(3) 
            C(8)-C(8A)-O(2A)             62(5) 
            C(7)-C(8A)-O(2A)            142(3) 
            O(2)-C(8A)-O(2A)             47.5(14) 
            C(9A)-C(9)-C(10)             38(8) 
            C(9A)-C(9)-O(2)              98(5) 
            C(10)-C(9)-O(2)             121.4(6) 
            C(9A)-C(9)-O(2A)             57(6) 
            C(10)-C(9)-O(2A)             91.4(7) 
            O(2)-C(9)-O(2A)              44.4(5) 
            C(9)-C(9A)-C(10)            124(10) 
            C(9)-C(9A)-O(2A)            103(10) 
            C(10)-C(9A)-O(2A)           126(10) 
            C(9)-C(9A)-O(2)              63(6) 
            C(10)-C(9A)-O(2)            139(7) 
            O(2A)-C(9A)-O(2)             44(2) 
            C(9A)-C(10)-C(9)             18(6) 
            C(9A)-C(10)-O(3)            116(4) 
            C(9)-C(10)-O(3)             112.3(6) 
            O(3)-C(11)-C(12)            107.9(5) 
            O(4A)-C(12)-C(11)           113.4(6) 
            O(4A)-C(12)-O(4)             38.9(5) 
            C(11)-C(12)-O(4)            109.7(6) 
            C(13A)-C(13)-O(4A)           81.1(14) 
            C(13A)-C(13)-O(4)            41.9(9) 
            O(4A)-C(13)-O(4)             50.2(10) 
            C(13A)-C(13)-C(14)           78(2) 
            O(4A)-C(13)-C(14)           152.1(17) 
            O(4)-C(13)-C(14)            102.3(18) 
            O(4)-C(13A)-C(13)            84(2) 
            O(4)-C(13A)-O(4A)            46.2(13) 
            C(13)-C(13A)-O(4A)           52.3(14) 
            O(4)-C(13A)-C(14)           114.7(19) 
            C(13)-C(13A)-C(14)           58.8(18) 
            O(4A)-C(13A)-C(14)          108.9(13) 
            C(13)-C(14)-O(5)            138.5(10) 
            C(13)-C(14)-C(13A)           42.8(7) 
            O(5)-C(14)-C(13A)            99.0(7) 
            C(3)-O(1)-C(7)              120.1(3) 
            O(2A)-O(2)-C(8)              60.9(8) 
            O(2A)-O(2)-C(8A)             70.2(18) 
            C(8)-O(2)-C(8A)              21.4(14) 
            O(2A)-O(2)-C(9)              72.5(8) 
            C(8)-O(2)-C(9)              111.5(8) 
            C(8A)-O(2)-C(9)             131.9(16) 
            O(2A)-O(2)-C(9A)             55(4) 
            C(8)-O(2)-C(9A)             104(3) 
            C(8A)-O(2)-C(9A)            121(3) 
            C(9)-O(2)-C(9A)              20(4) 
            O(2)-O(2A)-C(8)              68.7(9) 
            O(2)-O(2A)-C(9A)             81(5) 
            C(8)-O(2A)-C(9A)            128(6) 
            O(2)-O(2A)-C(8A)             62(2) 
            C(8)-O(2A)-C(8A)             20.3(13) 
            C(9A)-O(2A)-C(8A)           138(6) 
            O(2)-O(2A)-C(9)              63.1(8) 
            C(8)-O(2A)-C(9)             110.2(10) 
            C(9A)-O(2A)-C(9)             20(6) 
            C(8A)-O(2A)-C(9)            118(2) 
            C(11)-O(3)-C(10)            114.1(6) 
            C(13A)-O(4)-O(4A)            96.8(19) 
            C(13A)-O(4)-C(13)            54.2(16) 
            O(4A)-O(4)-C(13)             57.8(12) 
            C(13A)-O(4)-C(12)           116.2(18) 
            O(4A)-O(4)-C(12)             49.4(9) 
            C(13)-O(4)-C(12)            104.5(16) 
            O(4)-O(4A)-C(13)             72.0(10) 
            O(4)-O(4A)-C(12)             91.7(12) 
            C(13)-O(4A)-C(12)           153.3(17) 
            O(4)-O(4A)-C(13A)            36.9(8) 
            C(13)-O(4A)-C(13A)           46.5(9) 
            C(12)-O(4A)-C(13A)          108.3(12) 
            C(4)-O(5)-C(14)             115.3(3) 
            C(116)-C(111)-C(112)        117.9(3) 
            C(116)-C(111)-P             121.9(3) 
            C(112)-C(111)-P             120.2(2) 
            C(113)-C(112)-C(111)        119.8(3) 
            C(113)-C(112)-C             120.2(3) 
            C(111)-C(112)-C             120.0(3) 
            C(114)-C(113)-C(112)        120.8(3) 
            C(113)-C(114)-C(115)        119.7(3) 
            C(114)-C(115)-C(116)        120.4(3) 
            C(111)-C(116)-C(115)        121.3(3) 
            C(122)-C(121)-C(126)        117.4(3) 
            C(122)-C(121)-P             116.8(3) 
            C(126)-C(121)-P             125.7(3) 
            C(123)-C(122)-C(121)        121.0(4) 
            C(124)-C(123)-C(122)        120.4(4) 
            C(125)-C(124)-C(123)        120.1(4) 
            C(124)-C(125)-C(126)        119.9(4) 
            C(125)-C(126)-C(121)        121.2(4) 
            C(136)-C(131)-C(132)        118.0(3) 
            C(136)-C(131)-P             124.0(2) 
            C(132)-C(131)-P             117.9(3) 
            C(133)-C(132)-C(131)        121.5(4) 
            C(134)-C(133)-C(132)        120.0(4) 
            C(133)-C(134)-C(135)        119.3(4) 
            C(134)-C(135)-C(136)        120.9(4) 
            C(131)-C(136)-C(135)        120.3(3) 
           _____________________________________________________________ 
  
           Symmetry transformations used to generate equivalent atoms: 
            
  
    Table 4.  Anisotropic displacement parameters (A^2 x 10^3) for AMB3. 
    The anisotropic displacement factor exponent takes the form: 
    -2 pi^2 [ h^2 a*^2 U11 + ... + 2 h k a* b* U12 ] 
  
    _______________________________________________________________________ 
  
              U11        U22        U33        U23        U13        U12 
    _______________________________________________________________________ 
  
    P        59(1)      51(1)      50(1)      -1(1)       7(1)       8(1) 
    N        61(2)      66(2)      62(2)       4(2)      14(2)      14(2) 
    C        57(2)      56(2)      62(2)       9(2)      10(2)      14(2) 
    C(1)     60(2)      64(2)      50(2)       9(2)       9(2)      10(2) 
    C(2)     55(2)      73(2)      57(2)      -4(2)       9(2)       7(2) 
    C(3)     57(2)      73(2)      58(2)       2(2)       9(2)      14(2) 
    C(4)     77(3)      62(2)      50(2)      -1(2)      10(2)       8(2) 
    C(5)     65(3)      85(3)      60(2)       4(2)       0(2)       9(2) 
    C(6)     62(2)      84(3)      58(2)       7(2)       9(2)      21(2) 
    C(7)     76(3)     127(4)      83(3)     -13(3)      12(3)      39(3) 
    C(8)     63(4)     104(6)      66(6)       5(5)     -10(4)      36(5) 
    C(8A)   390(70)    280(50)    130(30)    -50(30)   -190(40)    220(40) 
    C(9)     76(4)     133(7)      92(5)     -15(5)       1(4)      66(5) 
    C(9A)  2000(400)  1200(200)   900(200)   800(200)  1100(300)  1500(300) 
    C(10)   195(7)     142(6)     166(7)      56(6)      61(6)      89(6) 
    C(11)   185(6)      67(3)     170(6)     -20(4)      59(5)       3(4) 
    C(12)   207(7)     101(5)     132(5)     -25(4)      32(5)      15(5) 
    C(13)   101(11)    108(13)    340(40)    100(20)     -5(15)    -27(11) 
    C(13A)  115(10)    137(15)    101(10)    -31(11)     55(10)    -12(9) 
    C(14)   141(5)     132(5)     106(4)     -49(4)      46(4)     -16(4) 
    O(1)     66(2)     135(2)      77(2)     -32(2)      -2(2)      33(2) 
    O(2)     95(3)      99(4)      82(4)       9(3)      23(3)      29(3) 
    O(2A)    95(8)     102(9)     108(10)     20(8)      34(7)      23(7) 
    O(3)    165(3)      91(2)     113(3)      17(2)      39(2)      25(2) 
    O(4)    119(7)     115(7)     133(8)     -21(7)      25(8)      -6(6) 
    O(4A)   112(6)      60(5)     129(6)     -18(4)      73(5)      15(4) 
    O(5)     94(2)      81(2)      65(2)      -8(2)      16(2)      10(1) 
    C(111)   58(2)      46(2)      47(2)       6(2)       4(2)      17(2) 
    C(112)   54(2)      45(2)      56(2)       7(2)       6(2)      15(2) 
    C(113)   62(2)      59(2)      74(2)      12(2)      14(2)      13(2) 
    C(114)   77(3)      46(2)      81(3)       4(2)       4(2)       4(2) 
    C(115)   82(3)      47(2)      66(2)      -2(2)       9(2)      15(2) 
    C(116)   71(2)      51(2)      55(2)       4(2)       9(2)      13(2) 
    C(121)   55(2)      49(2)      53(2)      -4(2)       2(2)       4(2) 
    C(122)   65(2)      72(2)      70(2)       0(2)       4(2)      14(2) 
    C(123)   65(3)      91(3)     101(4)     -15(3)      -1(3)      24(2) 
    C(124)   64(3)     106(3)     109(4)     -29(3)      27(3)      15(3) 
    C(125)   84(3)      94(3)      79(3)     -11(2)      33(3)       5(3) 
    C(126)   67(3)      70(2)      65(2)       1(2)      15(2)      11(2) 
    C(131)   60(2)      43(2)      57(2)       0(2)      13(2)       9(2) 
    C(132)   82(3)      52(2)      84(3)       2(2)       0(2)       5(2) 
    C(133)  107(3)      48(2)     115(4)      12(2)       7(3)      13(2) 
    C(134)   93(3)      67(3)      95(3)      26(2)      12(3)      30(2) 
    C(135)   86(3)      71(3)      81(3)      10(2)      -5(2)      17(2) 
    C(136)   81(3)      48(2)      69(2)       1(2)       1(2)      12(2) 
    _______________________________________________________________________ 
  
         Table 5.  Hydrogen coordinates ( x 10^4) and isotropic 
         displacement parameters (A^2 x 10^3) for AMB3. 
  
         ________________________________________________________________ 
  
                         x             y             z           U(eq) 
         ________________________________________________________________ 
  
          H(0B)        -954          6012          8717          70 
          H(2A)       -4613          6138          9387          76 
          H(5A)        -636          7884         11642          87 
          H(6A)        -520          6311         10402          82 
          H(7A)       -5882          7734          9228         116 
          H(7B)       -6607          6960          9890         116 
          H(8A)       -7973          8518          9404          96 
          H(8B)       -6757          9545          9839          96 
          H(8AA)      -7515          7902         10353         360 
          H(8AB)      -7397          8619          9462         360 
          H(9A)       -8676         10094         10352         122 
          H(9B)       -8857          9560         11317         122 
          H(9AA)      -8141         10642         10485        1339 
          H(9AB)      -8428          9600         11177        1339 
          H(10A)      -8108         11507         11710         190 
          H(10B)      -6844         11250         11277         190 
          H(11A)      -5182         11771         12651         168 
          H(11F)      -6181         12186         13299         168 
          H(12A)      -5519         10320         14131         180 
          H(12B)      -4546         11553         14450         180 
          H(13A)      -4483          8571         13607         228 
          H(13B)      -5054          9155         12624         228 
          H(13A)      -4422         10146         12296         140 
          H(13B)      -3085         10579         13114         140 
          H(14A)      -3625          7790         12487         155 
          H(14B)      -2535          8666         13231         155 
          H(11B)      -2961          3072          7894          77 
          H(11C)      -2774          1626          6611          85 
          H(11D)      -1013          1975          5774          79 
          H(11E)        428          3873          6151          71 
          H(12C)       3147          4883          8236          85 
          H(12D)       5040          4394          7622         107 
          H(12E)       5269          4967          6096         112 
          H(12F)       3600          5997          5142         102 
          H(12G)       1640          6401          5700          81 
          H(13C)       1113          8664          7513          91 
          H(13D)         98         10117          6514         111 
          H(13E)      -1737          9471          5181         101 
          H(13F)      -2541          7355          4844          99 
          H(13G)      -1482          5880          5808          82 
         ________________________________________________________________ 
  
         Table 6.  Torsion angles [deg] for AMB3. 
         ________________________________________________________________ 
  
          C(1)-N-C-C(112)                                     178.2(3) 
          C-N-C(1)-C(6)                                       -43.0(4) 
          C-N-C(1)-C(2)                                       138.5(3) 
          C(6)-C(1)-C(2)-C(3)                                   4.2(5) 
          N-C(1)-C(2)-C(3)                                   -177.3(3) 
          C(1)-C(2)-C(3)-O(1)                                 175.3(3) 
          C(1)-C(2)-C(3)-C(4)                                  -4.5(5) 
          O(1)-C(3)-C(4)-C(5)                                -177.4(3) 
          C(2)-C(3)-C(4)-C(5)                                   2.4(5) 
          O(1)-C(3)-C(4)-O(5)                                  -1.9(5) 
          C(2)-C(3)-C(4)-O(5)                                 177.9(3) 
          O(5)-C(4)-C(5)-C(6)                                -175.5(3) 
          C(3)-C(4)-C(5)-C(6)                                   0.0(6) 
          C(2)-C(1)-C(6)-C(5)                                  -1.7(5) 
          N-C(1)-C(6)-C(5)                                    179.9(3) 
          C(4)-C(5)-C(6)-C(1)                                  -0.4(6) 
          O(1)-C(7)-C(8)-C(8A)                                -54(9) 
          C(8A)-C(7)-C(8)-O(2A)                                53(9) 
          O(1)-C(7)-C(8)-O(2A)                                 -0.9(13) 
          C(8A)-C(7)-C(8)-O(2)                                 -2(8) 
          O(1)-C(7)-C(8)-O(2)                                 -56.6(9) 
          O(2A)-C(8)-C(8A)-C(7)                              -136(7) 
          O(2)-C(8)-C(8A)-C(7)                                178(8) 
          O(2A)-C(8)-C(8A)-O(2)                                46.6(18) 
          C(7)-C(8)-C(8A)-O(2)                               -178(8) 
          O(2)-C(8)-C(8A)-O(2A)                               -46.6(19) 
          C(7)-C(8)-C(8A)-O(2A)                               136(7) 
          O(1)-C(7)-C(8A)-C(8)                                129(8) 
          O(1)-C(7)-C(8A)-O(2)                                -55(6) 
          C(8)-C(7)-C(8A)-O(2)                                176(14) 
          O(1)-C(7)-C(8A)-O(2A)                                31(6) 
          C(8)-C(7)-C(8A)-O(2A)                               -98(12) 
          O(2)-C(9)-C(9A)-C(10)                              -133(8) 
          O(2A)-C(9)-C(9A)-C(10)                             -152(15) 
          C(10)-C(9)-C(9A)-O(2A)                              152(15) 
          O(2)-C(9)-C(9A)-O(2A)                                19(7) 
          C(10)-C(9)-C(9A)-O(2)                               133(8) 
          O(2A)-C(9)-C(9A)-O(2)                               -19(7) 
          O(2A)-C(9A)-C(10)-C(9)                             -145(17) 
          O(2)-C(9A)-C(10)-C(9)                               -86(16) 
          C(9)-C(9A)-C(10)-O(3)                                82(12) 
          O(2A)-C(9A)-C(10)-O(3)                              -63(10) 
          O(2)-C(9A)-C(10)-O(3)                                -4(15) 
          O(2)-C(9)-C(10)-C(9A)                                58(11) 
          O(2A)-C(9)-C(10)-C(9A)                               23(12) 
          C(9A)-C(9)-C(10)-O(3)                              -106(12) 
          O(2)-C(9)-C(10)-O(3)                                -48.3(10) 
          O(2A)-C(9)-C(10)-O(3)                               -83.0(8) 
          O(3)-C(11)-C(12)-O(4A)                               44.6(9) 
          O(3)-C(11)-C(12)-O(4)                                86.4(7) 
          O(4A)-C(13)-C(13A)-O(4)                              37.2(16) 
          C(14)-C(13)-C(13A)-O(4)                            -123.8(18) 
          O(4)-C(13)-C(13A)-O(4A)                             -37.2(16) 
          C(14)-C(13)-C(13A)-O(4A)                           -161.0(13) 
          O(4A)-C(13)-C(13A)-C(14)                            161.0(13) 
          O(4)-C(13)-C(13A)-C(14)                             123.8(18) 
          C(13A)-C(13)-C(14)-O(5)                             -29(2) 
          O(4A)-C(13)-C(14)-O(5)                              -73(4) 
          O(4)-C(13)-C(14)-O(5)                               -64(2) 
          O(4A)-C(13)-C(14)-C(13A)                            -43(3) 
          O(4)-C(13)-C(14)-C(13A)                             -34.6(10) 
          O(4)-C(13A)-C(14)-C(13)                              65(2) 
          O(4A)-C(13A)-C(14)-C(13)                             15.8(13) 
          O(4)-C(13A)-C(14)-O(5)                             -134(2) 
          C(13)-C(13A)-C(14)-O(5)                             160.9(16) 
          O(4A)-C(13A)-C(14)-O(5)                             176.7(11) 
          C(2)-C(3)-O(1)-C(7)                                 -14.7(6) 
          C(4)-C(3)-O(1)-C(7)                                 165.1(4) 
          C(8A)-C(7)-O(1)-C(3)                               -173(2) 
          C(8)-C(7)-O(1)-C(3)                                -161.3(5) 
          C(8A)-C(8)-O(2)-O(2A)                               111(5) 
          C(7)-C(8)-O(2)-O(2A)                                112.4(9) 
          O(2A)-C(8)-O(2)-C(8A)                              -111(5) 
          C(7)-C(8)-O(2)-C(8A)                                  1(5) 
          C(8A)-C(8)-O(2)-C(9)                                165(5) 
          O(2A)-C(8)-O(2)-C(9)                                 53.9(9) 
          C(7)-C(8)-O(2)-C(9)                                 166.3(6) 
          C(8A)-C(8)-O(2)-C(9A)                               146(7) 
          O(2A)-C(8)-O(2)-C(9A)                                35(5) 
          C(7)-C(8)-O(2)-C(9A)                                147(5) 
          C(8)-C(8A)-O(2)-O(2A)                               -60(5) 
          C(7)-C(8A)-O(2)-O(2A)                               123(6) 
          C(7)-C(8A)-O(2)-C(8)                               -177(10) 
          O(2A)-C(8A)-O(2)-C(8)                                60(5) 
          C(8)-C(8A)-O(2)-C(9)                                -19(6) 
          C(7)-C(8A)-O(2)-C(9)                                164(4) 
          O(2A)-C(8A)-O(2)-C(9)                                41.1(18) 
          C(8)-C(8A)-O(2)-C(9A)                               -39(7) 
          C(7)-C(8A)-O(2)-C(9A)                               144(7) 
          O(2A)-C(8A)-O(2)-C(9A)                               21(5) 
          C(9A)-C(9)-O(2)-O(2A)                               -23(10) 
          C(10)-C(9)-O(2)-O(2A)                               -54.4(10) 
          C(9A)-C(9)-O(2)-C(8)                                -70(10) 
          C(10)-C(9)-O(2)-C(8)                               -102.2(9) 
          O(2A)-C(9)-O(2)-C(8)                                -47.8(8) 
          C(9A)-C(9)-O(2)-C(8A)                               -63(10) 
          C(10)-C(9)-O(2)-C(8A)                               -95(2) 
          O(2A)-C(9)-O(2)-C(8A)                               -40(2) 
          C(10)-C(9)-O(2)-C(9A)                               -32(10) 
          O(2A)-C(9)-O(2)-C(9A)                                23(10) 
          C(9)-C(9A)-O(2)-O(2A)                               153(12) 
          C(10)-C(9A)-O(2)-O(2A)                              -96(15) 
          C(9)-C(9A)-O(2)-C(8)                                115(9) 
          C(10)-C(9A)-O(2)-C(8)                              -133(12) 
          O(2A)-C(9A)-O(2)-C(8)                               -38(4) 
          C(9)-C(9A)-O(2)-C(8A)                               129(8) 
          C(10)-C(9A)-O(2)-C(8A)                             -120(12) 
          O(2A)-C(9A)-O(2)-C(8A)                              -24(5) 
          C(10)-C(9A)-O(2)-C(9)                               111(16) 
          O(2A)-C(9A)-O(2)-C(9)                              -153(12) 
          C(8A)-O(2)-O(2A)-C(8)                                21.2(14) 
          C(9)-O(2)-O(2A)-C(8)                               -127.9(8) 
          C(9A)-O(2)-O(2A)-C(8)                              -137(5) 
          C(8)-O(2)-O(2A)-C(9A)                               137(5) 
          C(8A)-O(2)-O(2A)-C(9A)                              158(5) 
          C(9)-O(2)-O(2A)-C(9A)                                 9(5) 
          C(8)-O(2)-O(2A)-C(8A)                               -21.2(14) 
          C(9)-O(2)-O(2A)-C(8A)                              -149.1(14) 
          C(9A)-O(2)-O(2A)-C(8A)                             -158(5) 
          C(8)-O(2)-O(2A)-C(9)                                127.9(8) 
          C(8A)-O(2)-O(2A)-C(9)                               149.1(14) 
          C(9A)-O(2)-O(2A)-C(9)                                -9(5) 
          C(8A)-C(8)-O(2A)-O(2)                               -68(6) 
          C(7)-C(8)-O(2A)-O(2)                                -93.7(10) 
          C(8A)-C(8)-O(2A)-C(9A)                             -126(7) 
          O(2)-C(8)-O(2A)-C(9A)                               -59(4) 
          C(7)-C(8)-O(2A)-C(9A)                              -153(4) 
          O(2)-C(8)-O(2A)-C(8A)                                68(6) 
          C(7)-C(8)-O(2A)-C(8A)                               -26(6) 
          C(8A)-C(8)-O(2A)-C(9)                              -116(6) 
          O(2)-C(8)-O(2A)-C(9)                                -48.6(8) 
          C(7)-C(8)-O(2A)-C(9)                               -142.2(8) 
          C(9)-C(9A)-O(2A)-O(2)                               -24(10) 
          C(10)-C(9A)-O(2A)-O(2)                              127(8) 
          C(9)-C(9A)-O(2A)-C(8)                                30(12) 
          C(10)-C(9A)-O(2A)-C(8)                             -179(5) 
          O(2)-C(9A)-O(2A)-C(8)                                54(3) 
          C(9)-C(9A)-O(2A)-C(8A)                                5(14) 
          C(10)-C(9A)-O(2A)-C(8A)                             156(6) 
          O(2)-C(9A)-O(2A)-C(8A)                               29(5) 
          C(10)-C(9A)-O(2A)-C(9)                              151(16) 
          O(2)-C(9A)-O(2A)-C(9)                                24(10) 
          C(8)-C(8A)-O(2A)-O(2)                               104(6) 
          C(7)-C(8A)-O(2A)-O(2)                              -131(5) 
          C(7)-C(8A)-O(2A)-C(8)                               125(10) 
          O(2)-C(8A)-O(2A)-C(8)                              -104(6) 
          C(8)-C(8A)-O(2A)-C(9A)                               70(9) 
          C(7)-C(8A)-O(2A)-C(9A)                             -164(6) 
          O(2)-C(8A)-O(2A)-C(9A)                              -33(6) 
          C(8)-C(8A)-O(2A)-C(9)                                72(6) 
          C(7)-C(8A)-O(2A)-C(9)                              -162(4) 
          O(2)-C(8A)-O(2A)-C(9)                               -31.2(14) 
          C(9A)-C(9)-O(2A)-O(2)                               153(11) 
          C(10)-C(9)-O(2A)-O(2)                               136.0(8) 
          C(9A)-C(9)-O(2A)-C(8)                              -156(11) 
          C(10)-C(9)-O(2A)-C(8)                              -172.4(10) 
          O(2)-C(9)-O(2A)-C(8)                                 51.5(9) 
          C(10)-C(9)-O(2A)-C(9A)                              -17(11) 
          O(2)-C(9)-O(2A)-C(9A)                              -153(11) 
          C(9A)-C(9)-O(2A)-C(8A)                             -176(11) 
          C(10)-C(9)-O(2A)-C(8A)                              166.9(18) 
          O(2)-C(9)-O(2A)-C(8A)                                30.9(16) 
          C(12)-C(11)-O(3)-C(10)                             -169.6(5) 
          C(9A)-C(10)-O(3)-C(11)                              142(6) 
          C(9)-C(10)-O(3)-C(11)                               161.7(6) 
          C(13)-C(13A)-O(4)-O(4A)                             -41.6(15) 
          C(14)-C(13A)-O(4)-O(4A)                             -93(2) 
          O(4A)-C(13A)-O(4)-C(13)                              41.6(15) 
          C(14)-C(13A)-O(4)-C(13)                             -52(2) 
          C(13)-C(13A)-O(4)-C(12)                             -89(2) 
          O(4A)-C(13A)-O(4)-C(12)                             -47.8(14) 
          C(14)-C(13A)-O(4)-C(12)                            -140.9(10) 
          O(4A)-C(13)-O(4)-C(13A)                            -129(2) 
          C(14)-C(13)-O(4)-C(13A)                              56(2) 
          C(13A)-C(13)-O(4)-O(4A)                             129(2) 
          C(14)-C(13)-O(4)-O(4A)                             -174.7(17) 
          C(13A)-C(13)-O(4)-C(12)                             112.1(19) 
          O(4A)-C(13)-O(4)-C(12)                              -16.8(12) 
          C(14)-C(13)-O(4)-C(12)                              168.5(9) 
          O(4A)-C(12)-O(4)-C(13A)                              76(2) 
          C(11)-C(12)-O(4)-C(13A)                             -27(2) 
          C(11)-C(12)-O(4)-O(4A)                             -103.1(10) 
          O(4A)-C(12)-O(4)-C(13)                               18.8(14) 
          C(11)-C(12)-O(4)-C(13)                              -84.4(16) 
          C(13A)-O(4)-O(4A)-C(13)                              39.5(17) 
          C(12)-O(4)-O(4A)-C(13)                              158.4(13) 
          C(13A)-O(4)-O(4A)-C(12)                            -118.9(17) 
          C(13)-O(4)-O(4A)-C(12)                             -158.4(13) 
          C(13)-O(4)-O(4A)-C(13A)                             -39.5(17) 
          C(12)-O(4)-O(4A)-C(13A)                             118.9(17) 
          C(13A)-C(13)-O(4A)-O(4)                             -31.7(14) 
          C(14)-C(13)-O(4A)-O(4)                               11(4) 
          C(13A)-C(13)-O(4A)-C(12)                             23(3) 
          O(4)-C(13)-O(4A)-C(12)                               55(3) 
          C(14)-C(13)-O(4A)-C(12)                              66(5) 
          O(4)-C(13)-O(4A)-C(13A)                              31.7(14) 
          C(14)-C(13)-O(4A)-C(13A)                             43(3) 
          C(11)-C(12)-O(4A)-O(4)                               92.8(11) 
          C(11)-C(12)-O(4A)-C(13)                              42(3) 
          O(4)-C(12)-O(4A)-C(13)                              -51(3) 
          C(11)-C(12)-O(4A)-C(13A)                             59.2(13) 
          O(4)-C(12)-O(4A)-C(13A)                             -33.6(10) 
          C(13)-C(13A)-O(4A)-O(4)                             124(2) 
          C(14)-C(13A)-O(4A)-O(4)                             106(2) 
          O(4)-C(13A)-O(4A)-C(13)                            -124(2) 
          C(14)-C(13A)-O(4A)-C(13)                            -17.1(12) 
          O(4)-C(13A)-O(4A)-C(12)                              67.2(18) 
          C(13)-C(13A)-O(4A)-C(12)                           -169.2(15) 
          C(14)-C(13A)-O(4A)-C(12)                            173.6(9) 
          C(5)-C(4)-O(5)-C(14)                               -111.8(5) 
          C(3)-C(4)-O(5)-C(14)                                 72.7(5) 
          C(13)-C(14)-O(5)-C(4)                              -130.4(13) 
          C(13A)-C(14)-O(5)-C(4)                             -150.0(8) 
          C(121)-P-C(111)-C(116)                              -15.7(3) 
          C(131)-P-C(111)-C(116)                               90.0(3) 
          C(121)-P-C(111)-C(112)                              162.9(2) 
          C(131)-P-C(111)-C(112)                              -91.4(3) 
          C(116)-C(111)-C(112)-C(113)                           1.0(4) 
          P-C(111)-C(112)-C(113)                             -177.7(2) 
          C(116)-C(111)-C(112)-C                              179.7(3) 
          P-C(111)-C(112)-C                                     1.1(4) 
          N-C-C(112)-C(113)                                    -4.5(5) 
          N-C-C(112)-C(111)                                   176.7(3) 
          C(111)-C(112)-C(113)-C(114)                          -1.0(5) 
          C-C(112)-C(113)-C(114)                             -179.8(3) 
          C(112)-C(113)-C(114)-C(115)                          -0.3(5) 
          C(113)-C(114)-C(115)-C(116)                           1.5(5) 
          C(112)-C(111)-C(116)-C(115)                           0.3(4) 
          P-C(111)-C(116)-C(115)                              178.9(2) 
          C(114)-C(115)-C(116)-C(111)                          -1.5(5) 
          C(131)-P-C(121)-C(122)                              166.9(3) 
          C(111)-P-C(121)-C(122)                              -87.3(3) 
          C(131)-P-C(121)-C(126)                               -9.6(3) 
          C(111)-P-C(121)-C(126)                               96.2(3) 
          C(126)-C(121)-C(122)-C(123)                          -0.8(5) 
          P-C(121)-C(122)-C(123)                             -177.6(3) 
          C(121)-C(122)-C(123)-C(124)                           0.4(6) 
          C(122)-C(123)-C(124)-C(125)                          -0.4(6) 
          C(123)-C(124)-C(125)-C(126)                           0.8(6) 
          C(124)-C(125)-C(126)-C(121)                          -1.3(6) 
          C(122)-C(121)-C(126)-C(125)                           1.3(5) 
          P-C(121)-C(126)-C(125)                              177.8(3) 
          C(121)-P-C(131)-C(136)                               94.4(3) 
          C(111)-P-C(131)-C(136)                              -11.6(3) 
          C(121)-P-C(131)-C(132)                              -88.0(3) 
          C(111)-P-C(131)-C(132)                              165.9(3) 
          C(136)-C(131)-C(132)-C(133)                          -1.9(6) 
          P-C(131)-C(132)-C(133)                             -179.6(3) 
          C(131)-C(132)-C(133)-C(134)                           1.6(7) 
          C(132)-C(133)-C(134)-C(135)                          -1.0(7) 
          C(133)-C(134)-C(135)-C(136)                           0.8(6) 
          C(132)-C(131)-C(136)-C(135)                           1.7(5) 
          P-C(131)-C(136)-C(135)                              179.3(3) 
          C(134)-C(135)-C(136)-C(131)                          -1.2(6) 
         ________________________________________________________________ 
  
         Symmetry transformations used to generate equivalent atoms: 
          
  
 Table 7.  Hydrogen bonds for AMB3 [A and deg.]. 
 ____________________________________________________________________________ 
  
 D-H...A                      d(D-H)      d(H...A)    d(D...A)    <(DHA) 
  
